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Tài liệu Experimental study on strength and permeability of pervious concrete pavement containing fly ash, blast furnace slag and silica fume

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VIETNAM NATIONAL UNIVERSITY, HANOI VIETNAM JAPAN UNIVERSITY TRAN THANH TUAN EXPERIMENTAL STUDY ON STRENGTH AND PERMEABILITY OF PERVIOUS CONCRETE PAVEMENT USING FLY ASH, BLAST FURNACE SLAG AND SILICAFUME MASTER’S THESIS Hanoi, 2019 VIETNAM NATIONAL UNIVERSITY, HANOI VIETNAM JAPAN UNIVERSITY TRAN THANH TUAN EXPERIMENTAL STUDY ON STRENGTH AND PERMEABILITY OF PERVIOUS CONCRETE PAVEMENT USING FLY ASH, BLAST FURNACE SLAG AND SILICAFUME MAJOR: MASTER IN INFRASTRUCTURE ENGINEERING CODE: RESEARCH SUPERVISOR: Associate Prof. Dr. KOHEI NAGAI Dr. DUONG QUANG HUNG Hanoi, 2019 CONTENTS Acknowledgment ....................................................................................................... 6 Abstract ...................................................................................................................... 7 LIST OF FIGURE .................................................................................................... 3 LIST OF TABLE ...................................................................................................... 4 LIST OF ABBREVIATIONS .................................................................................. 5 CHAPTER 1: INTRODUCTION ............................................................................ 6 1.1. Background of Pervious Concrete Pavement ........................................... 8 1.2. Scope and Objective .................................................................................... 9 CHAPTER 2: LITTERATURE REVIEW ........................................................... 10 2.1. Introduction of the development of pervious concrete .......................... 10 2.2. Overview of pervious concrete uses Fly ash and BFS additives ........... 12 CHAPTER 3: METHODOLOGY AND EXPERIMENT ................................... 15 3.1. Methodology ............................................................................................... 15 3.2. Experimental procedure ........................................................................... 15 3.2.1. Compressive and flexural strength test. ................................................... 15 3.2.2. Void ratio test. .......................................................................................... 15 3.3. Matertial preparation ............................................................................... 17 3.4. Mixing Proportions and Casting Specimen ............................................ 24 3.4.1. Proportion ................................................................................................. 24 3.4.2. Casting Specimen ..................................................................................... 25 CHAPTER 4: RESULTS AND DISCUSSION .................................................... 28 4.1. RESULTS ................................................................................................... 28 4.1.1. Compressive Strength of PCPC ............................................................... 28 4.1.2. Permeability of PCPC: ............................................................................. 31 4.2. 4.2.1. Discussion ................................................................................................... 33 Combine slag in slurry to make porous concrete ..................................... 33 1 4.2.2. 4.2.3. Mortar with BFS and SF produces strength pervious concrete ................ 34 Fly ash particle did not significantly enhance strength of porous concrete 35 CHAPTER 5: CONCLUSION AND RECOMMENDATION ........................... 37 5.1. Conclusion .................................................................................................. 37 5.2. Recommendation ....................................................................................... 38 Reference.................................................................................................................. 39 2 LIST OF FIGURE Figure 3.1: Mixing PCPC with concrete mixer ................................................... 25 Figure 3.2: Casting specimen at Lab .................................................................... 25 Figure 3.4: Curing PCPC specimen at Lab ......................................................... 27 Figure 4.1: Testing PCPC at Lab .......................................................................... 28 Figure 4.2: The PCPC sample is destroyed after compression .......................... 29 Figure 4.3: Crack of PCPC after compression .................................................... 29 Figure 4.4: Compressive strength development with time ................................. 30 Figure 4.5: Testing permeability of PCPC ........................................................... 31 Figure 4.6: Void ratio (%) of PCPC Specimen.........Error! Bookmark not defined. Figure 4.7: Coefficient of Permeability (mm/s) ................................................... 33 Figure 4.8: Hydrated Cement Paste ..................................................................... 34 Figure 4.9: Cement Hydration Reaction .............................................................. 34 Figure 4.10: Pozzolanic Reaction .......................................................................... 35 Figure 5.1: solution for designing PCPC road structure layers......................... 38 3 LIST OF TABLE Table 2.1: Summary of the research results on PCPC ....................................... 10 Table 2.2: Typical mix design and properties of existing PCPC in the US (reported by Nation Ready Mix Concrete Association – NRMCA, 2004) ......................... 11 Table 3.1. Physical and chemical properties of OPC and GGBS ...................... 17 Table 3.2: Mix Proportion of specimens in trial experiment ............................. 24 Table 4.1: Compressive strength of PCPC .......................................................... 30 Table 4.2: Void ratio of PCPC .............................................................................. 29 Table 4.3: Permeability of PCPC .......................................................................... 29 4 LIST OF ABBREVIATIONS PCPC : Portland cement Pervious Concrete PCP : Pervious Concrete Pavement NRMACA : National Mixing Concrete Association SP : Super plasticizer SF : Silica Fume FA : Fly Ash BFS : Blast Furnace Slag GGBFS : Ground Granulated Blast Furnace Slag CSH : Calcium Silicate Hydrate AASHTO : American Association of State Highway and Transportation Officials ACI : American Concrete Institute ASTM : American Society for Testing and Materials FHWA : Federal Highway Administration - United States Department of Transportation ACPA : American Concrete Pavement Association NRMCA : Nation Ready Mix Concrete Association 5 Acknowledgment My master thesis was started from my internship at The University of Tokyo in September 2018. It was really a memorable and lucky time in my life. Experimental activities at Komaba Campus – The University of Tokyo are very interesting and useful during the internship in Japan under the supervision of Associate Professor Kohei Nagai - University of Tokyo, Japan and Dr. Duong Quang Hung - Hanoi Architectural University. From the bottom of my heart, I would like to express my gratitude to Associate Professor Kohei Nagai, Dr. Duong Quang Hung for giving me helpful advice and dedicated guidance and valuable lectures for conducting research. It is difficult to express my gratitude to two talented and respectable professors Professor Nguyen Dinh Duc - Vietnam National University in Hanoi and Professor Hironori Kato – University of Tokyo. Two co-directors of the Master in Infrastructure Engineering program - VJU gave me useful advice and orientation in the right direction. Also, I would like to send many thanks to Dr. Phan Le Binh, lecturer, JICA long term expert who always encouraged me and Dr. Tien Dung Nguyen Dung at VJU for his devoted and valuable support. Their support is extremely precious and always inspires me to complete the thesis. Also, without the help of my friends studying at Komaba Campus - University of Tokyo, I would not have accomplished my thesis. Therefore, I would like to thank for their help. The last, I would like to give special thanks to MIE02-VJU classmates and students from the same course at Vietnam Japan University for supporting and accompanying me throughout my great time at Vietnam Japan University. My master thesis is also a gift for my whole family, for my parents, my wife and my lovely children because they were always beside me during the whole time I studied at VJU. Sincerely, Tran Thanh Tuan 6 ABSTRACT About 30 years ago, Porous Concrete (PC) was studied for use in the United Kingdom and the United States in some traffic works. In Europe and Japan, to reduce noise and improve skid resistance, PC is also used as a very effective application material. Research and application development of Blast Furnace Slag (BFS) are widely used in Portland Cement Pervious Concrete (PCPC).Fly ash (FA) is very important because it not only increases the surface drainage capacity of transport works but also contributes to reducing pollution as a material of environmental friendliness. According to a study in Belgium, for some PC mixtures, the 28-day compressive strength also reaches 31.7 MPa. However, the permeability of this mixture has not been specifically reported. Therefore, research on PCPC strength and permeability with the use of BFS, FA to replace part of cement and to achieve proper permeability is very promising and essential in the future. PCPC is a kind of concrete mixture made from coarse aggregate, small sand content (0-20% by weight of aggregate or no sand, water from 27-43% and binder. Pervious concrete with void ratio of 14-30% and rough textured surface. In this study, the author has found some mixing proportion of porous concrete using BFS and FA to replace part of cement and reduce the amount of sand used. The author carried out the design of various mixing proportion used for PC such as ash, flying ash combined with silica fume. The experimental process at the Komaba Lab - Tokyo University finds the results and compares the effect of each of these materials on the strength and permeability of PC. When using BFS in combination with silica fume, the mixed concrete resulted in a strength of porous concrete of 29.42 MPa with a permeability of 1,747 mm / s. It can be considered for application in a number of projects using porous concrete that can drain in reality such as parking lots, sidewalks, etc. 7 CHAPTER 1: INTRODUCTION 1.1. Background of Pervious Concrete Pavement Today, along with the development of modern construction technologies, advanced and environmentally friendly materials are also focused on sustainable development. Concrete is a common construction material in the construction industry in general and technical infrastructure in particular. In particular, Portland Cement Pervious Concrete (PCPC) or Pervious Concrete Pavement (PCP) is a material that has been researched and applied in recently as an environmentally friendly material. According to the National Mixing Concrete Association (NRMCA), porous concrete is a high porosity concrete used for flat surface concrete applications that allows water from rain and other sources to flow through. This will reduce the flow from one location and reload the groundwater level. These are also called non-fines concrete and are made of Portland cement, coarse aggregates, water, with little or no sand and additives. The draining water PCP has many merits, such as good safety driving in rainy days, reducing noise, high anti-slippery performance of the pavement and no accumulated water, no splash and spray in rainy days, increasing the driving safety in rainy days greatly. The draining water bituminous pavement obtains widespread applications in Western Europe, US and Japan and so on. Porous concrete is used for pavement materials, it can penetrate rainwater at the source, contributing to improved driving safety, noise while reducing traffic, road heat effects in the capital. Marketing is also overcome and contributes to sustainable development. Evaluating the environmental impact of porous concrete with non-porous or conventional concrete also gives different results. Porous pavement makes air, water and temperature penetrate into different parts of the environment, from which they undergo different storage, handling and flow processes. Therefore, porous concrete is an environmentally friendly material. 8 Research on using fly ash and Blast Furnace Slag also contributes to reducing environmental pollution because Blast Furnace Slag pollutes water and air when left in nature. 1.2. Scope and Objective Objectives: The study on strength and permeability of PC containing fly ash, slag and silica fume is to achieve the following goals: - To investigate the effect of fly ash and Blast furnace slag, silica fume on strength and permeability of PCPC - To achieve PCPC mixture design that has necessary compressive strength and permeability suitable for practical road applications. Scope: Pervious concrete pavement has important indicators as strength, permeability, abrasion, surface texture and some other indicators. Within the scope of this thesis, the author focuses on two main indicators: strength and permeability of Pervious Concrete Pavement (PCP). The super plasticizer used in this study is a common polycarboxylate-based SP8P admixture in Japan, which increases the workability, slump for concrete and extends the setting time of cement and concrete. Experimental process of making PCP samples at Komaba Lab, the study carried out the design, tested the compressive strength of concrete according to ACI 522 standard and determined the permeability of PCP according to Park and Tia’s Equation (2004). By using materials to replace a part of cement such as Blast Furnace Slag (BFS), Fly Ash (FA) with additives such as Super plasticizer (SP) and Silica Fume (SF) to find the optimal mixture. PCPC has enough strength and permeability to be applied in practice. Structure of thesis: Chapter 1: Introduction Chapter 2: Literature review Chapter 3: Methodology and Experiment Chapter 4: Result and discussion. Chapter 5: Recommendation and conclusion. 9 CHAPTER 2: LITTERATURE REVIEW 2.1. Introduction of the development of pervious concrete Leading institutes and associations in the field of concrete pavement in the world:  United States Department of Transportation – Federal Highway Administration (FHWA)  American Concrete Pavement Association (ACPA)  American Association of State Highway and Transportation Officials (AASHTO)  ACI Committee 522 – Pervious Concrete  Center for Transportation Research and Education, Iowa State University The issues around PCPC have been investigated as the following table: Table 2.1 Summary of the research results on PCPC No Issues 1 Construction Materials 2 PCPC Material Properties 3 Researcher Tennis (2004); Tamai (2003); Kajio (1998). Strength Kaijo (1998); Beeldens (2003); Tennis (2004); Elsayed (2011) Porosity and permeability Ferguson(2005); Tennis (2004); Yang (2003) Tanaka (1998) Surface Characteristics Noise reduction Olek (2003); Tamai (2003) 4 Pervious Pavement Design Kosmatra (2002); Young (2005); Ramadhansyah (2014) 5 Construction Husain (2015), Darshna shar (2013), 6 Maintenance Olek (2003) 7 Environment PCP using waste material Durability of Porous Concrete Sukamal (2015) Tamai (2003) An Experimental study on the water-purification properties Park, Tia (2004) of porous concrete 10 According to research, author Nguyen Van Chanh pointed out that: Pervious Concrete is a type of concrete with continuous pore structure, magnetic porosity (15-35%) having the same composition as normal concrete, however coarse aggregates are used with the same grain size and contain very little or no sand. (Nguyen Van Chanh et al., 2005). When using synthetic stone gravel with smaller size, it increases compressive strength, while increasing porosity in concrete structure and thus increasing the drainage capacity of porous concrete. However, the drainage capacity of porous concrete is not merely secondary to porosity, but is still dependent to many other factors such as continuous counting, winding, pore surface Water (W) and cement (C): The W/C ratio is determined to be from 0.25 to 0.45. Unlike conventional concrete, the amount of cement in porous concrete is lower than the amount of pore between aggregate particles. When the strength of cement mortar increases, it will lead to an increase in the overall strength of porous concrete. Therefore, it is necessary to control the amount of water closely. Using the right amount of water will make the concrete mixture get the desired properties, no mortar phenomenon will flow to the bottom of the bottom layer to fill the pores, causing the drainage of porous concrete. Pervious concrete mix designs in the US include cement, coarse aggregates with a size between 2.54 cm and No. 4 sieves and are classified according to the ratio of water/cement (W / C) within from 0.25 to 0.43. 28-day compressive strength of porous concrete ranged from 7 MPa – 24 MPa, with the rate of voids from 14% to 31% and the range of velocity permeability (2-6 cm/min). Compared to conventional concrete, compressive strength ranges from 3,500 to 4,000psi (28 MPa – 32 MPa), lower than 3,000 psi. Table 2.2 Typical mix design and properties of existing PCPC in the US (reported by Nation Ready Mix Concrete Association – NRMCA, 2004) Property Specification Cement content 300 to 600 lbs/yd3 Coarse aggregate content 2,400 to 180 to 360 kg/m3 2,700 1,440 to 1,620 kg/m3 11 Fine aggregate content lbs/yd3 0 kg/m3 Water-cement ratio 0 lbs/yd3 0.27 to 0.43 Aggregate to cement ratio 0.27 to 0.43 4 to 4.5/1 by mass Slump 0 to 1 inch 0 to 2.54 cm 28-day strength compressive 800 to 3,000 psi 1 to 3.8 MPa Flexural strength Void ratio Permeability (flow rate) 7 to 24 MPa 14% to 31% by volume 36 to inches/hour 864 2 to 36 cm/min (120 to 320 L/m2/min) Density (unit weight) 1600 to 2000 kg/m3 Shrinkage 200x10-6 Strength and permeability The Strength of concrete pavement is lower than that of conventional concrete. Therefore, the application of PCPC is limited to low-intensity structures such as parking lots, shoulder lanes, light traffic areas, or roads but not highways. For a wider application, a long-term plan for the study of porous concrete pavements is needed to determine the optimal porous concrete mixing ratio to enhance the strength with suitable permeability to be used highway or highway surface. Nader Ghafoori and Shivaji Dutta reported that both sealed- and wet-curing conditions have shown similar effects on strength development. Moreover, the gain in strength, under both curing types, is unaffected by the increase in compaction energy. It is found the strength of no-fine concrete increase with rise in compaction energy. The movement of water will be more convenient when the interconnected voids are present in the structure of the permeable concrete. When the porosity is higher, the texture is lower in strength and when the porosity is lower, the strength of the porous concrete will be higher (Ferguson, 2005). 2.2. Overview of pervious concrete uses Fly ash and BFS additives Pervious Concrete: ''The new era for rural road sidewalks'' has said: 12 The objective of the study is to evaluate the cost effectiveness of porous concrete compared to conventional concrete. In that study, conventional concrete was used according to the design of the IS Class M20, including 59.25 kg of cement (300 rs/50 kg), 88.88 kg of fine aggregate (600 rs/1 ton) and a total of 177.8 kg (1000 rs/1 ton) (Darshna et al., 2013). Pervious concrete is used in accordance with the NRMCA guidelines, which are composed of 46.5 kg of cement (300rs / 50kg) and concrete of course (1000rs /1 ton). The conclusion indicates that Porous concrete reduces the flow of rainwater to increase the amount of groundwater to eliminate costly storms for water management practices. And that is significant savings in the amount of about 29 rs/m3 or 18 rs/ft2. A study named: “Effect of Aggregate Grading and Cement By-Product on Performance of Pervious Concrete” also indicates that: Replacing part of cement with industrial by-products such as fly ash, GGBS has been successfully used as an additional cement material as the target of this study. The author used type 53 cement (specific weight 3.15), coarse aggregate (transmitted through 20 mm and left sieve on 10 mm sieve) together with using GGBS (specific gravity 2.88), fly ash and water (Husain et al., 2015). Through the research article named: "Evaluation of performance of absorbent concrete using waste materials”, the use of furnace slag, rice husk ash and silica fume and solid waste (glass powder, ceramic waste, bottom ash) and its effect on strong compressive strength and permeability are as per below: Usage: Fly ash (2-50%), RHA (10-30%), GGBS (35-70), Silica fume (8-12%), Rubber waste, Glass powder (20-40%) is used to replace part of cement. Research shows that the compressive strength and permeability when using materials have different effects as below: Fly ash gives long-term compressive strength when increasing but then decreases compressive strength. Rice husk ash reduces more than 10-12% of compressive strength, permeability and durability. 13 GGBFS gives higher strength but lower permeability. Silica fume increases compressive strength but does not affect permeability. Glass powder strengthens durability and workability and Ceramic powder improves durability (Sukamal et al., 2015). Author A.Elsayed in the research paper: "Influence of Silica Fume, Fly Ash, Super Pozz and high slag on water permeability and strength of concrete" said that: Can improve the properties of concrete, such as increasing resistance and reducing permeability by using mineral additives such as fly ash, BFS and silica fume. (Elsayed, 2011). Conclusion In previous studies, increasing the strength of porous concrete will lead to reduce permeability and vice versa. In the data sheet you can see, the PCPC strength is about 7-31 MPa. That is the limit to expand the application of porous concrete in practice. Limitations on strength & durability prevent widespread application of Porous Concrete. 14 CHAPTER 3: METHODOLOGY 3.1. Methodology Topics using experimental methods to research. The steps for conducting the study include: The calculation of grading using cement, coarse aggregates, fine aggregates with FA, BFS replaces part of cement, SP and SF as additives based on ACI 522 standard and inherits pervious research results. After that, casting samples and testing the strength and permeability of PCPC are conducted. 3.2. Experimental procedure Experiment method: There are four types of tests to characterize properties of pervious concrete mix in this research, including unconfined compressive strength, flexural strength, void ratio and permeability. The characterization of tests methods and formulas used for the experiment are indicated as following: 3.2.1. Compressive and flexural strength test. Slump of the fresh concrete is measured following ASTM C143 by a standard cone test. Compressive strength is determined according to ASTM C39, and flexural strength is conducted in accordance with ASTM C78 (using simple beam with third-point loading). The cylinder specimens with 10cm in diameter and 20cm in length are used for testing compressive strength. The prismatic samples 10x10x40cm are for testing flexural strength. Testing machine to test the compressive strength of samples with a capacity of 100 tons is used, cylindrical test samples are aged at 7, 28, 56, 91 days since casting. Loading speed is 14 N /mm2/minute. 3.2.2. Void ratio test. The void ratio of pervious concrete is determined by measuring the weight difference between dry samples and water saturated samples. When using the equation of Park and Tia (2004), cylindrical samples with a diameter of 10cm and a length of 20 cm were constructed to check the void ratio: 15   W  W1  100(%) Vr  1   2    wVol  where, (1) Vr: total void ratio, % W1: weight under water, kg W2: oven dry weight, kg Vol: volume of sample, cm3  w: density of water, kg/cm3 Permeability test The samples are wrapped in rubber and surrounded by adjustable tube clamps. Cylindrical sample for experiments has a diameter of 10cm and a height of 20 cm. The average permeability coefficient (k) is determined as follows according to Das equation (1998): k aL  h0  ln   At  ht  where, (2) k: coefficient of permeability, cm/sec a: area of standpipe, cm2 L: height of sample, cm A: area of sample, cm2 t: time for water to drop from h0 to ht, sec h0: height of water in burette at initial time (t = 0), cm ht: height of water in burette at final time (t = t), cm 16 3.3. Material preparation Material: Ordinary Portland cement (C), Fly Ash (FA) ash, blast furnace slag (BFS) and silica fume (SF) are used in this study. Crushed gravel with the largest size Dmax 15mm used as a raw aggregate, washed with water before use (G) Super-plasticizer (SP, a sulfoanated naphthalene formaldehyde condensate of Japanese origin, a dark brown aqueous solution with 42% solids and a density of 1.2) is employed to aid the dispersion of Nano-particles and silica in binder and achieve good workability of concrete. 20% sand to coarse aggregate by mass is used, which is expected to enhance strength of pervious concrete. Cement Ordinary Portland cement (OPC) follows JIS R5210 standard, used in this study. The physical properties and chemical properties as well as the limit value are specified by JIS R5210. Ground Granulated Blast Furnace Slag (GGBFS) or Blast Furnace Slag (BFS) Blast furnace slag (GGBS) or blast furnace slag (BFS), is used instead of OPC in this study. Blast furnace slag conforms to JIS A6206 and the criteria listed in Table 3.1. Table 3.1 Physical and chemical properties of OPC and GGBS OPC Material JIS R5210 Physical properties Density, cm3 Fineness, g/ GGBS4 OPC JIS A6202 GGBS - 3.15 < 2.80 2.91 > 2500 3470 3000- 4070 17 cm2/g 5000 LOI < 3.0 0.77 < 0.3 - SiO2 - 20.84 - - Al2O3 - 5.95 - - Fe2O3 - 2.62 - - CaO - 63.63 - - MgO < 5.0 1.79 < 10.0 5.46 SO3 < 3.0 1.97 - 0.04 Na2O - 0.18 < 4.0 - K2O - 0.33 - - TiO2 - 0.34 - - P2O5 - 0.08 - - MnO - 0.1 - - CI < 0.02 ND < 0.02 0.005 Chemical properties Note: “-“: not be specified, “ND”: not be determined Fly ash In the process of burning coal in power plants with by-products produced, it is fly ash. Helmuth (Mindes and Young) has shown a summary of the properties and chemical composition of different fly ash. Based on the chemical composition, it is classified as fly ash type F or type C. In type F there is a lower amount of High, hence less cement properties and vice versa, C has higher CaO content, so it has more cement properties and less toxic than F-type fly ash (Elsayed, 2011). 18
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